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LiquidNitrogenCryostat-Optics

Liquid Nitrogen Cryostat - Optics

Working principle

 

The low-pressure refrigerant is introduced into the cryostat from the liquid inlet, and then introduced into the evaporator at the bottom of the cryostat through the capillary tube inside the cryostat. A heater and a temperature sensor are also installed on the evaporator of the cryostat. , the steam whose temperature is controlled by the temperature controller is sprayed into the sample chamber. After cooling the sample, the steam is discharged through the air outlet pipe into the atmosphere or into a gas recovery device. In the design of this type of cryostat, in order to facilitate customers to easily load samples, the sample can be loaded from the top of the cryostat through the sample rod. The bottom of the cryostat uses a compact design with a vacuum cover. has a smaller duty cycle and is more suitable for measurements in magnetic fields.

 

Features:


◆ Temperature range (65K~500K), (optional 700K), high efficiency and fast cooling speed;
◆ The sample is in the vacuum chamber, providing an ideal and stable experimental environment;
◆ The vacuum interlayer is equipped with low-temperature adsorbent, which can increase the vacuum holding time and extend the use time of liquid nitrogen;
◆ The temperature sensor uses PT100 platinum resistor with good stability and repeatability;
◆ Multiple options to meet different testing needs;
◆ It is convenient to add liquid nitrogen during use;
◆ The optical sample holder can be equipped with a pluggable sample card and easy-to-use and beautiful binding posts;
◆ Can be customized according to customer requirements;
◆ Comes with 8 measuring leads as standard, which can be expanded to 32;
◆ The window comes standard with 2 fused quartz windows, which can be expanded to 5, and the window material can be changed according to user requirements;
◆ Changing samples is quick and convenient, and can be completed within 5 minutes;
◆ The sample holder is available as liquid sample holder, dust sample holder, solid sample holder, and block sample holder.

 

Technical specifications

 

Model

DXT9115-4W

DXT9115-4W-H DXT9120-4W DXT9120-4W-H DXT9130-4W DXT9130-4W-H

Temperature range

65-325k

65-500k

65-325k

65-500k

65-325k

65-500k

Cooling time

≤25min

Optical window

Four Φ15X1.5

Four Φ20X1.5

Four Φ30X1.5

Test lead connector

Standard 8-core measurement lead connector, optional coaxial connector and microwave connector.     

Sample holder size

15X25mm

15X25mm 20X30mm 20X30mm 30X40mm 30X40mm

Thermometer

PT100 platinum resistance thermometer (both calibrated and uncalibrated, the default is uncalibrated)

Temperature stability

±0.01K depends on the DXTC-290 temperature controller

Heater

30W

60W 30W 60W 30W 60W

Vacuum interface

Standard KF25 interface

Sample environment

The sample is placed in a vacuum environment

Vacuum degree

≤1Pa is enough

Liquid nitrogen maintenance time

6h@80K; 5h@100K; 3h@200K

Liquid nitrogen chamber volume

Standard 500ml (can be customized)

Application scope

Spectral testing, photoelectric reaction, Raman, electroluminescence, photoluminescence, etc.

Note: Standard temperature range (80K~500K); expandable temperature range (65K~500K)

 

 

Sample holder options:

 

Model 

Specifications

Material

Describe

DXT9115-4W

15X25mm

OFHC

Standard optical sample holder,

DXT9115-4W-10LTH

15X25mm

OFHC

Standard optical sample holder with Φ10mm hole in the middle

DXT9115-4W-H-10LTH

15X25mm

OFHC

Standard optical sample holder with Φ10mm hole in the middle

DXT9120-4W

20X30mm

OFHC

Standard optical sample holder, no hole in the middle

DXT9120-4W-15LTH

20X30mm

OFHC

Standard optical sample holder with Φ15mm hole in the middle

DXT9120-4W-H-15LTH

20X30mm

OFHC

Standard optical sample holder with Φ15mm hole in the middle

DXT9130-4W

30X40mm

OFHC

Standard optical sample holder, no hole in the middle

DXT9130-4W-20LTH

30X40mm

OFHC

Standard optical sample holder with Φ20mm hole in the middle

DXT9130-4W-H-20LTH

30X40mm

OFHC

Standard optical sample holder with Φ20mm hole in the middle

DXPSC-10

Φ10

Quartz

Powder sample container with 10mm quartz window on one side

 

Remark:
 
1: All standard optical cryostats are shipped from the factory with only one sample holder.
2: If the above standard sample holder cannot meet customer needs, it can be customized according to customer requirements.
3: In order to fix the optical performance sample, all optical cryostats are equipped with a pressing plate to hold the sample. The aperture of the pressing plate is consistent with the size of the light hole.

 

 

Cryostat Optical connector options:

 

Electrical connector model

Specifications

Describe

DXT91-8P ordinary glass sintering

8pin

Add a quick-plug 8P ordinary electrical connector

DXT91-12P ordinary glass sintering

12pin

Add a quick-plug 12P ordinary electrical connector

DXT91-SMA

0-18GHz

With soft cable

0-12.4GHz

Equipped with semi-rigid and semi-flexible cables

DXT91-BNC

0-4GHz

With ordinary coaxial cable

DXT91-TRX

triax connector

Add a quick-plug triaxial connector

DXT91-S

Stainless steel junction box

Add a stainless steel junction box

DXT91-PTEF

PTFE wiring cover

Add a PTFE plate wiring cover to the stainless steel junction box

 

Remark:

 

1: When all cryostats leave the factory, they are equipped with two connectors. One is for the installation of temperature sensors and heaters, and the other is a connector prepared for other performance measurements. When more test lines are needed, you will need Add mounting holes or install one or more Breakout Boxes;
2: There is the DXT91-S option in the above table. The wiring board and the shell of this option are integrally connected to the ground. The other is the DXT91-PTEF option. This option uses PTFE board insulation in the shell and the installed connector. The electrical properties of the housing and connector are independent of each other. This issue should be paid attention to when selecting.
3: Pressure reduction accessory options. The standard cryostat itself does not come with special pressure reduction spare parts. When a low temperature of 65K is required, corresponding pressure reduction accessories need to be configured.

 

Liquid nitrogen thermostat - optics can be applied to spectrum testing, photoelectric reaction, Raman, electroluminescence, photoluminescence, etc.
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